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Determination of bisphenol A traces in water samples from the Vrbas River and its tributaries, Bosnia and Herzegovina

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2022
Determination_of_bisphenol_pub_2022.pdf (2.352Mb)
Authors
Savić, Dajana
Balaban, Milica
Pantelić, Nebojša
Savić, Dejana N.
Antić, Mališa
Dekić, Radoslav
Antić, Vesna
Article (Published version)
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Abstract
The bisphenol A (BPA) concentration was determined in 12 surface water samples of the Vrbas River and its five tributaries. The samples were taken in the area that belongs to the city of Banja Luka (Bosnia and Herzegovina). BPA was isolated using micro liquid-liquid extraction followed by derivatization and gas chromatography-mass spectrometry analysis (GC-MS). Silylation was used as a derivatization method to increase volatility and allow the GC-MS determination of BPA. The limits of detection (LOD) and quantification (LOQ), obtained by validating the procedure, were determined at 4 and 10 ng L-1, respectively. The concentrations of BPA were ranged between 33 and 354 ng L-1, and all were above the LOQ value. The lowest amount of BPA was found in the sample collected in the river Vrbas, near Švrakava estuary upstream from the city of Banja Luka. The highest concentration of BPA was recorded at the confluence of the Crkvena and Vrbas rivers, which is located in the city center. This stu...dy shows that population and human activity could affect the level of BPA in the environment.

Keywords:
Bisphenol A / Derivatization / GC-MS / Microextraction / River water
Source:
Journal of the Serbian Chemical Society, 2022, 87, 1, 109-119
Publisher:
  • Serbian Chemical Society
Funding / projects:
  • Ministry of Education, Science and Technological Development, Republic of Serbia, Grant no. 200116 (University of Belgrade, Faculty of Agriculture) (RS-200116)

DOI: 10.2298/JSC211001098S

ISSN: 0352-5139

WoS: 000744024900001

Scopus: 2-s2.0-85124496026
[ Google Scholar ]
URI
http://aspace.agrif.bg.ac.rs/handle/123456789/6015
Collections
  • Radovi istraživača / Researchers’ publications
Institution/Community
Poljoprivredni fakultet
TY  - JOUR
AU  - Savić, Dajana
AU  - Balaban, Milica
AU  - Pantelić, Nebojša
AU  - Savić, Dejana N.
AU  - Antić, Mališa
AU  - Dekić, Radoslav
AU  - Antić, Vesna
PY  - 2022
UR  - http://aspace.agrif.bg.ac.rs/handle/123456789/6015
AB  - The bisphenol A (BPA) concentration was determined in 12 surface water samples of the Vrbas River and its five tributaries. The samples were taken in the area that belongs to the city of Banja Luka (Bosnia and Herzegovina). BPA was isolated using micro liquid-liquid extraction followed by derivatization and gas chromatography-mass spectrometry analysis (GC-MS). Silylation was used as a derivatization method to increase volatility and allow the GC-MS determination of BPA. The limits of detection (LOD) and quantification (LOQ), obtained by validating the procedure, were determined at 4 and 10 ng L-1, respectively. The concentrations of BPA were ranged between 33 and 354 ng L-1, and all were above the LOQ value. The lowest amount of BPA was found in the sample collected in the river Vrbas, near Švrakava estuary upstream from the city of Banja Luka. The highest concentration of BPA was recorded at the confluence of the Crkvena and Vrbas rivers, which is located in the city center. This study shows that population and human activity could affect the level of BPA in the environment.
PB  - Serbian Chemical Society
T2  - Journal of the Serbian Chemical Society
T1  - Determination of bisphenol A traces in water samples from the Vrbas River and its tributaries, Bosnia and Herzegovina
EP  - 119
IS  - 1
SP  - 109
VL  - 87
DO  - 10.2298/JSC211001098S
ER  - 
@article{
author = "Savić, Dajana and Balaban, Milica and Pantelić, Nebojša and Savić, Dejana N. and Antić, Mališa and Dekić, Radoslav and Antić, Vesna",
year = "2022",
abstract = "The bisphenol A (BPA) concentration was determined in 12 surface water samples of the Vrbas River and its five tributaries. The samples were taken in the area that belongs to the city of Banja Luka (Bosnia and Herzegovina). BPA was isolated using micro liquid-liquid extraction followed by derivatization and gas chromatography-mass spectrometry analysis (GC-MS). Silylation was used as a derivatization method to increase volatility and allow the GC-MS determination of BPA. The limits of detection (LOD) and quantification (LOQ), obtained by validating the procedure, were determined at 4 and 10 ng L-1, respectively. The concentrations of BPA were ranged between 33 and 354 ng L-1, and all were above the LOQ value. The lowest amount of BPA was found in the sample collected in the river Vrbas, near Švrakava estuary upstream from the city of Banja Luka. The highest concentration of BPA was recorded at the confluence of the Crkvena and Vrbas rivers, which is located in the city center. This study shows that population and human activity could affect the level of BPA in the environment.",
publisher = "Serbian Chemical Society",
journal = "Journal of the Serbian Chemical Society",
title = "Determination of bisphenol A traces in water samples from the Vrbas River and its tributaries, Bosnia and Herzegovina",
pages = "119-109",
number = "1",
volume = "87",
doi = "10.2298/JSC211001098S"
}
Savić, D., Balaban, M., Pantelić, N., Savić, D. N., Antić, M., Dekić, R.,& Antić, V.. (2022). Determination of bisphenol A traces in water samples from the Vrbas River and its tributaries, Bosnia and Herzegovina. in Journal of the Serbian Chemical Society
Serbian Chemical Society., 87(1), 109-119.
https://doi.org/10.2298/JSC211001098S
Savić D, Balaban M, Pantelić N, Savić DN, Antić M, Dekić R, Antić V. Determination of bisphenol A traces in water samples from the Vrbas River and its tributaries, Bosnia and Herzegovina. in Journal of the Serbian Chemical Society. 2022;87(1):109-119.
doi:10.2298/JSC211001098S .
Savić, Dajana, Balaban, Milica, Pantelić, Nebojša, Savić, Dejana N., Antić, Mališa, Dekić, Radoslav, Antić, Vesna, "Determination of bisphenol A traces in water samples from the Vrbas River and its tributaries, Bosnia and Herzegovina" in Journal of the Serbian Chemical Society, 87, no. 1 (2022):109-119,
https://doi.org/10.2298/JSC211001098S . .

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