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The influence of thermodynamic parameters of the alkaline activator on the mechanical properties of geopolymers

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2019
Ivanovic_18YRC.pdf (3.192Mb)
Authors
Ivanović, Marija D.
Đukić, Dunja
Mladenović, Nataša
Kljajević, Ljiljana M.
Pavlović, Vladimir
Nenadović, Snežana S.
Mirković, Miljana M.
Conference object (Published version)
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Abstract
In order to optimize process of geopolymerization, the investigation of thermodynamic parameters of alkali activators are important. The aim of this research was to investigate the influence of thermodynamic parameters (density, viscosity, refractive index and sound velocity) of alkaline activators on mechanical properties (compressive strength and hardness) of synthesized geopolymer samples. Geopolymers were synthetized by alkaline activation of metakaolin, having the density 2.524 g/cm3, using the activators at elevated temperature of 60 oC for two days. Based on the obtained results thermodynamic properties has been selected to predict the properties of materials. Four series of alkaline activators have been used. Activators remarked as AA1, AA2, AA3 and AA4 present the mixtures of Na2SiO3 and solutions of NaOH, of different molarities 2M, 4M, 6M and 8M respectively. The volume ratio of Na2SiO3 and aqueous solution of NaOH was the same for all samples. Densities, viscosities and ref...ractive indices of alkaline activators were determined over the temperature range 15-60 oC of process of geopolymerizations. The values of density, viscosity and refractive index decrease with temperature increase over the investigated temperature range. Increasing molarity of alkali activator solutions, the sound velocity of activators is changed. For sample AA2 the values of sound velocity rises from room temperature to 45 °C and then begins to decrease while for the sample AA3 sound velocity grows until 30 °C and then starts to decrease with further increasing of temperature. Four series of geopolymer samples GP1 to GP4 were synthesiyed using the constant ratio of solid and liquid phase. FTIR, XRD, SEM-EDS methods were used for physicochemical further characterization of geopolymer samples.

Keywords:
geopolymerization / alkaline activators / geopolymers / thermodynamic parameters / mechanical properties
Source:
Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia, 2019, 87-87
Publisher:
  • Belgrade : Institute of Technical Sciences of SASA
Funding / projects:
  • Synthesis, processing and characterization of nanostructured materials for application in the field of energy, mechanical engineering, environmental protection and biomedicine (RS-45012)

ISBN: 978-86-80321-35-6

[ Google Scholar ]
Handle
https://hdl.handle.net/21.15107/rcub_dais_6965
URI
http://dais.sanu.ac.rs/123456789/6965
http://aspace.agrif.bg.ac.rs/handle/123456789/5746
Collections
  • Radovi istraživača / Researchers’ publications
Institution/Community
Poljoprivredni fakultet
TY  - CONF
AU  - Ivanović, Marija D.
AU  - Đukić, Dunja
AU  - Mladenović, Nataša
AU  - Kljajević, Ljiljana M.
AU  - Pavlović, Vladimir
AU  - Nenadović, Snežana S.
AU  - Mirković, Miljana M.
PY  - 2019
UR  - http://dais.sanu.ac.rs/123456789/6965
UR  - http://aspace.agrif.bg.ac.rs/handle/123456789/5746
AB  - In order to optimize process of geopolymerization, the investigation of thermodynamic parameters of alkali activators are important. The aim of this research was to investigate the influence of thermodynamic parameters (density, viscosity, refractive index and sound velocity) of alkaline activators on mechanical properties (compressive strength and hardness) of synthesized geopolymer samples. Geopolymers were synthetized by alkaline activation of metakaolin, having the density 2.524 g/cm3, using the activators at elevated temperature of 60 oC for two days. Based on the obtained results thermodynamic properties has been selected to predict the properties of materials. Four series of alkaline activators have been used. Activators remarked as AA1, AA2, AA3 and AA4 present the mixtures of Na2SiO3 and solutions of NaOH, of different molarities 2M, 4M, 6M and 8M respectively. The volume ratio of Na2SiO3 and aqueous solution of NaOH was the same for all samples. Densities, viscosities and refractive indices of alkaline activators were determined over the temperature range 15-60 oC of process of geopolymerizations. The values of density, viscosity and refractive index decrease with temperature increase over the investigated temperature range. Increasing molarity of alkali activator solutions, the sound velocity of activators is changed. For sample AA2 the values of sound velocity rises from room temperature to 45 °C and then begins to decrease while for the sample AA3 sound velocity grows until 30 °C and then starts to decrease with further increasing of temperature. Four series of geopolymer samples GP1 to GP4 were synthesiyed using the constant ratio of solid and liquid phase. FTIR, XRD, SEM-EDS methods were used for physicochemical further characterization of geopolymer samples.
PB  - Belgrade : Institute of Technical Sciences of SASA
C3  - Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia
T1  - The influence of thermodynamic parameters of the alkaline activator on the mechanical properties of geopolymers
EP  - 87
SP  - 87
UR  - https://hdl.handle.net/21.15107/rcub_dais_6965
ER  - 
@conference{
author = "Ivanović, Marija D. and Đukić, Dunja and Mladenović, Nataša and Kljajević, Ljiljana M. and Pavlović, Vladimir and Nenadović, Snežana S. and Mirković, Miljana M.",
year = "2019",
abstract = "In order to optimize process of geopolymerization, the investigation of thermodynamic parameters of alkali activators are important. The aim of this research was to investigate the influence of thermodynamic parameters (density, viscosity, refractive index and sound velocity) of alkaline activators on mechanical properties (compressive strength and hardness) of synthesized geopolymer samples. Geopolymers were synthetized by alkaline activation of metakaolin, having the density 2.524 g/cm3, using the activators at elevated temperature of 60 oC for two days. Based on the obtained results thermodynamic properties has been selected to predict the properties of materials. Four series of alkaline activators have been used. Activators remarked as AA1, AA2, AA3 and AA4 present the mixtures of Na2SiO3 and solutions of NaOH, of different molarities 2M, 4M, 6M and 8M respectively. The volume ratio of Na2SiO3 and aqueous solution of NaOH was the same for all samples. Densities, viscosities and refractive indices of alkaline activators were determined over the temperature range 15-60 oC of process of geopolymerizations. The values of density, viscosity and refractive index decrease with temperature increase over the investigated temperature range. Increasing molarity of alkali activator solutions, the sound velocity of activators is changed. For sample AA2 the values of sound velocity rises from room temperature to 45 °C and then begins to decrease while for the sample AA3 sound velocity grows until 30 °C and then starts to decrease with further increasing of temperature. Four series of geopolymer samples GP1 to GP4 were synthesiyed using the constant ratio of solid and liquid phase. FTIR, XRD, SEM-EDS methods were used for physicochemical further characterization of geopolymer samples.",
publisher = "Belgrade : Institute of Technical Sciences of SASA",
journal = "Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia",
title = "The influence of thermodynamic parameters of the alkaline activator on the mechanical properties of geopolymers",
pages = "87-87",
url = "https://hdl.handle.net/21.15107/rcub_dais_6965"
}
Ivanović, M. D., Đukić, D., Mladenović, N., Kljajević, L. M., Pavlović, V., Nenadović, S. S.,& Mirković, M. M.. (2019). The influence of thermodynamic parameters of the alkaline activator on the mechanical properties of geopolymers. in Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia
Belgrade : Institute of Technical Sciences of SASA., 87-87.
https://hdl.handle.net/21.15107/rcub_dais_6965
Ivanović MD, Đukić D, Mladenović N, Kljajević LM, Pavlović V, Nenadović SS, Mirković MM. The influence of thermodynamic parameters of the alkaline activator on the mechanical properties of geopolymers. in Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia. 2019;:87-87.
https://hdl.handle.net/21.15107/rcub_dais_6965 .
Ivanović, Marija D., Đukić, Dunja, Mladenović, Nataša, Kljajević, Ljiljana M., Pavlović, Vladimir, Nenadović, Snežana S., Mirković, Miljana M., "The influence of thermodynamic parameters of the alkaline activator on the mechanical properties of geopolymers" in Program and the Book of abstracts / Eighteenth Young Researchers' Conference Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia (2019):87-87,
https://hdl.handle.net/21.15107/rcub_dais_6965 .

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