Application of Novel Sorbents in D-Μ-Spe Sample Preparation for Gc-Ms Analysis of Pahs in Water
Primena novih sorbenasa u D-µ-SPE TEhnici pripreme uzoraka za GC – MS analizu PAU u vodi

2018
Authors
Ćirić, SlobodanStankov-Jovanović, Vesna
Mitić, Violeta
Ilić, Marija
Jovanović, Snežana
Stojanović, Gordana
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The aim of this paper is application of novel sorbents in dispersive micro solid phase extraction (D-μ-SPE) as a technique for sample preparation of water, for the analysis of 16 PAHs by gass chromatography - mass spectrometry (GC-MS). D-μ-SPE proved to be an effective technique consuming a small amount of the solvent for the analysis. D-μ-SPE is characterized by its rapidity (7 minutes per sample including all preparation of standard solutions and measuring of sorbents) and cheapness as well. Low values of the detection limit and limit of quantification, acceptable accuracy and precision values propose this method for routine water analysis for the determination of PAHs.
Cilj istraživanja ovog rada je primena novih sorbenasa u disperzivnoj mikroekstrakciji čvrstom fazom (D-µ-SPE) kao tehnikom pripreme uzoraka vode za analizu 16 prioritetnih PAU gasnom hromatografijom sa masenom spektrometrijom (GC-MS). D-µ-SPE se pokazala kao efikasna i ekonomična tehnika pripreme uzoraka vode pri čemu se troši mala količina rastvarača za ekstrakciju i koristi jeftin pribor za pripremu uzoraka koja traje 7 minuta (uključujući pripreme standardnih rastvora i odmeravanje sorbenasa). Niske vrednosti granice detekcije i kvantifikacije, prihvatljive vrednosti tačnosti i preciznosti predloženu metodu analize 16 prioritetnih PAU kvalifikujuje za rutinsku analizu vode.
Keywords:
GC-MS / D-μ-SPE / sorbents / PAHsSource:
23. Savetovanje o biotehnologiji sa međunarodnim učešćem, Čačak, 09.-10. 03. 2018., 2018Funding / projects:
- Natural products of plants and lichens: isolation, identification, biological activity and application (RS-172047)
- Development of new and improvement of existing electrochemical, spectroscopic and flow injection (FIA) methods on environmental quality monitoring (RS-172051)
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Poljoprivredni fakultetTY - CONF AU - Ćirić, Slobodan AU - Stankov-Jovanović, Vesna AU - Mitić, Violeta AU - Ilić, Marija AU - Jovanović, Snežana AU - Stojanović, Gordana PY - 2018 UR - http://aspace.agrif.bg.ac.rs/handle/123456789/5657 AB - The aim of this paper is application of novel sorbents in dispersive micro solid phase extraction (D-μ-SPE) as a technique for sample preparation of water, for the analysis of 16 PAHs by gass chromatography - mass spectrometry (GC-MS). D-μ-SPE proved to be an effective technique consuming a small amount of the solvent for the analysis. D-μ-SPE is characterized by its rapidity (7 minutes per sample including all preparation of standard solutions and measuring of sorbents) and cheapness as well. Low values of the detection limit and limit of quantification, acceptable accuracy and precision values propose this method for routine water analysis for the determination of PAHs. AB - Cilj istraživanja ovog rada je primena novih sorbenasa u disperzivnoj mikroekstrakciji čvrstom fazom (D-µ-SPE) kao tehnikom pripreme uzoraka vode za analizu 16 prioritetnih PAU gasnom hromatografijom sa masenom spektrometrijom (GC-MS). D-µ-SPE se pokazala kao efikasna i ekonomična tehnika pripreme uzoraka vode pri čemu se troši mala količina rastvarača za ekstrakciju i koristi jeftin pribor za pripremu uzoraka koja traje 7 minuta (uključujući pripreme standardnih rastvora i odmeravanje sorbenasa). Niske vrednosti granice detekcije i kvantifikacije, prihvatljive vrednosti tačnosti i preciznosti predloženu metodu analize 16 prioritetnih PAU kvalifikujuje za rutinsku analizu vode. C3 - 23. Savetovanje o biotehnologiji sa međunarodnim učešćem, Čačak, 09.-10. 03. 2018. T1 - Application of Novel Sorbents in D-Μ-Spe Sample Preparation for Gc-Ms Analysis of Pahs in Water T1 - Primena novih sorbenasa u D-µ-SPE TEhnici pripreme uzoraka za GC – MS analizu PAU u vodi UR - https://hdl.handle.net/21.15107/rcub_agrospace_5657 ER -
@conference{ author = "Ćirić, Slobodan and Stankov-Jovanović, Vesna and Mitić, Violeta and Ilić, Marija and Jovanović, Snežana and Stojanović, Gordana", year = "2018", abstract = "The aim of this paper is application of novel sorbents in dispersive micro solid phase extraction (D-μ-SPE) as a technique for sample preparation of water, for the analysis of 16 PAHs by gass chromatography - mass spectrometry (GC-MS). D-μ-SPE proved to be an effective technique consuming a small amount of the solvent for the analysis. D-μ-SPE is characterized by its rapidity (7 minutes per sample including all preparation of standard solutions and measuring of sorbents) and cheapness as well. Low values of the detection limit and limit of quantification, acceptable accuracy and precision values propose this method for routine water analysis for the determination of PAHs., Cilj istraživanja ovog rada je primena novih sorbenasa u disperzivnoj mikroekstrakciji čvrstom fazom (D-µ-SPE) kao tehnikom pripreme uzoraka vode za analizu 16 prioritetnih PAU gasnom hromatografijom sa masenom spektrometrijom (GC-MS). D-µ-SPE se pokazala kao efikasna i ekonomična tehnika pripreme uzoraka vode pri čemu se troši mala količina rastvarača za ekstrakciju i koristi jeftin pribor za pripremu uzoraka koja traje 7 minuta (uključujući pripreme standardnih rastvora i odmeravanje sorbenasa). Niske vrednosti granice detekcije i kvantifikacije, prihvatljive vrednosti tačnosti i preciznosti predloženu metodu analize 16 prioritetnih PAU kvalifikujuje za rutinsku analizu vode.", journal = "23. Savetovanje o biotehnologiji sa međunarodnim učešćem, Čačak, 09.-10. 03. 2018.", title = "Application of Novel Sorbents in D-Μ-Spe Sample Preparation for Gc-Ms Analysis of Pahs in Water, Primena novih sorbenasa u D-µ-SPE TEhnici pripreme uzoraka za GC – MS analizu PAU u vodi", url = "https://hdl.handle.net/21.15107/rcub_agrospace_5657" }
Ćirić, S., Stankov-Jovanović, V., Mitić, V., Ilić, M., Jovanović, S.,& Stojanović, G.. (2018). Application of Novel Sorbents in D-Μ-Spe Sample Preparation for Gc-Ms Analysis of Pahs in Water. in 23. Savetovanje o biotehnologiji sa međunarodnim učešćem, Čačak, 09.-10. 03. 2018.. https://hdl.handle.net/21.15107/rcub_agrospace_5657
Ćirić S, Stankov-Jovanović V, Mitić V, Ilić M, Jovanović S, Stojanović G. Application of Novel Sorbents in D-Μ-Spe Sample Preparation for Gc-Ms Analysis of Pahs in Water. in 23. Savetovanje o biotehnologiji sa međunarodnim učešćem, Čačak, 09.-10. 03. 2018.. 2018;. https://hdl.handle.net/21.15107/rcub_agrospace_5657 .
Ćirić, Slobodan, Stankov-Jovanović, Vesna, Mitić, Violeta, Ilić, Marija, Jovanović, Snežana, Stojanović, Gordana, "Application of Novel Sorbents in D-Μ-Spe Sample Preparation for Gc-Ms Analysis of Pahs in Water" in 23. Savetovanje o biotehnologiji sa međunarodnim učešćem, Čačak, 09.-10. 03. 2018. (2018), https://hdl.handle.net/21.15107/rcub_agrospace_5657 .