University of Belgrade - Faculty of Agriculture
AgroSpace - Faculty of Agriculture Repository
    • English
    • Српски
    • Српски (Serbia)
  • English 
    • English
    • Serbian (Cyrillic)
    • Serbian (Latin)
  • Login
View Item 
  •   AgroSpace
  • Poljoprivredni fakultet
  • Radovi istraživača / Researchers’ publications
  • View Item
  •   AgroSpace
  • Poljoprivredni fakultet
  • Radovi istraživača / Researchers’ publications
  • View Item
JavaScript is disabled for your browser. Some features of this site may not work without it.

Synthesis of BaTiO3 from a mechanically activated BaCO3-TiO2 system

Thumbnail
2008
1801.pdf (619.8Kb)
Authors
Pavlović, Vera P.
Stojanović, B.D.
Pavlović, Vladimir
Marinković-Stanojević, Z.
Živković, Lj.
Ristić, M.M.
Article (Published version)
Metadata
Show full item record
Abstract
In this article the solid state reaction of BaTiO3 formation from a mechanically activated BaCO3-TiO2 system has been investigated. An equimolar mixture of BaCO3 and TiO2 powders was activated in a planetary ball mill in a continual regime for 0, 30 and 90 min, pressed and thermally treated up to 1200°C. The effect of the milling and firing regime on the phase formation was investigated by the X-ray diffraction (XRD) method and differential thermal analysis (DTA). Deconvolution of the experimental DTA curve corresponding to the BaTiO3 synthesis process has been performed. The influence of the activation time on the change of characteristic temperature for each elementary step in the complete solid-state reaction of BaTiO3 formation, was analyzed. These results were correlated with the ones obtained by SEM characterization and by XRD analysis.
U ovome radu je analiziran uticaj mehaničke aktivacije sistema BaCO3- TiO2 na formiranje BaTiO3. Ekvimolarne smeše praha BaCO3 i TiO2 su aktivirane u planetarnom mlinu u kontinualnom režimu tokom 0, 30 i 90 min. Uzorci su zatim presovani i termički tretirani do 1200oC. Efekat mlevenja i zagrevanja na promene faza je analiziran primenom rendgenske fazne analize i diferencijalne termijske analize. Izvršena je dekonvolucija eksperimentalno dobijene DTA krive koja odgovara procesu sinteze BaTiO3, kao i analiza uticaja vremena aktivacije na promene karakteristične temperature za svaki pojedinačni elementarni proces tokom sinteze barijum titanata. Ovi rezultati su korelisani sa rezultatima dobijenim SEM i XRD analizom.
Keywords:
barium titanate / mechanical activation / sintering / barijum titanat / mehanička aktivacija / sinterovanje
Source:
Science of Sintering, 2008, 40, 1, 21-26
Publisher:
  • Međunarodni Institut za nauku o sinterovanju, Beograd
Funding / projects:
  • Investigation of the relation in triad: Synthesis structure-properties for functional materials (RS-142011)

DOI: 10.2298/SOS0801021P

ISSN: 0350-820X

WoS: 000255915700003

Scopus: 2-s2.0-70350254912
[ Google Scholar ]
URI
http://aspace.agrif.bg.ac.rs/handle/123456789/1804
Collections
  • Radovi istraživača / Researchers’ publications
Institution/Community
Poljoprivredni fakultet

DSpace software copyright © 2002-2015  DuraSpace
About the AgroSpace Repository | Send Feedback

re3dataOpenAIRERCUB
 

 

All of DSpaceCommunitiesAuthorsTitlesSubjectsThis institutionAuthorsTitlesSubjects

Statistics

View Usage Statistics

DSpace software copyright © 2002-2015  DuraSpace
About the AgroSpace Repository | Send Feedback

re3dataOpenAIRERCUB