TY  - JOUR
AU  - Tomić, Nataša Z.
AU  - Vuksanović, Marija M.
AU  - Djokić, Veljko
AU  - Mitrić, Miodrag
AU  - Simić, Milena R.
AU  - Pavlović, Vladimir
AU  - Jancić-Heinemann, Radmila
AU  - Marinković, Aleksandar D.
PY  - 2019
UR  - http://aspace.agrif.bg.ac.rs/handle/123456789/5002
AB  - A facile synthesis was employed for three polyhedral oligo silsequioxanes (POSS), obtaining incompletely condensed structures with fern-like and cubic morphologies. Proton nuclear magnetic resonance spectroscopy (H-1 NMR) indicated the successful synthesis of the proposed POSS structures. The hydroxyl groups affected the manner and type of POSS morphology, as seen under a scanning electron microscope (SEM) and a transmission electron microscope (TEM). Fourier-transform infrared spectroscopy (FTIR) showed the availability of surface hydroxyl groups that contributed to the formation of a higher amount of char residue, as found from TGA analysis. The highest decomposition temperature (281 degrees C) and the least char residue were found for a cross-linkable POSS, obtained by esterification of the hydroxyl groups with methacryloyl chloride.
PB  - Pergamon-Elsevier Science Ltd, Oxford
T2  - Polyhedron
T1  - Synthesis and characterization of nanocrystalline polyhedral oligo silsesquioxanes (POSS) with cross-linkable functionalities
EP  - 304
SP  - 299
VL  - 171
DO  - 10.1016/j.poly.2019.06.059
ER  - 

@article{
author = "Tomić, Nataša Z. and Vuksanović, Marija M. and Djokić, Veljko and Mitrić, Miodrag and Simić, Milena R. and Pavlović, Vladimir and Jancić-Heinemann, Radmila and Marinković, Aleksandar D.",
year = "2019",
abstract = "A facile synthesis was employed for three polyhedral oligo silsequioxanes (POSS), obtaining incompletely condensed structures with fern-like and cubic morphologies. Proton nuclear magnetic resonance spectroscopy (H-1 NMR) indicated the successful synthesis of the proposed POSS structures. The hydroxyl groups affected the manner and type of POSS morphology, as seen under a scanning electron microscope (SEM) and a transmission electron microscope (TEM). Fourier-transform infrared spectroscopy (FTIR) showed the availability of surface hydroxyl groups that contributed to the formation of a higher amount of char residue, as found from TGA analysis. The highest decomposition temperature (281 degrees C) and the least char residue were found for a cross-linkable POSS, obtained by esterification of the hydroxyl groups with methacryloyl chloride.",
publisher = "Pergamon-Elsevier Science Ltd, Oxford",
journal = "Polyhedron",
title = "Synthesis and characterization of nanocrystalline polyhedral oligo silsesquioxanes (POSS) with cross-linkable functionalities",
pages = "304-299",
volume = "171",
doi = "10.1016/j.poly.2019.06.059"
}

Tomić, N. Z., Vuksanović, M. M., Djokić, V., Mitrić, M., Simić, M. R., Pavlović, V., Jancić-Heinemann, R.,& Marinković, A. D.. (2019). Synthesis and characterization of nanocrystalline polyhedral oligo silsesquioxanes (POSS) with cross-linkable functionalities. in Polyhedron
Pergamon-Elsevier Science Ltd, Oxford., 171, 299-304.
https://doi.org/10.1016/j.poly.2019.06.059

Tomić NZ, Vuksanović MM, Djokić V, Mitrić M, Simić MR, Pavlović V, Jancić-Heinemann R, Marinković AD. Synthesis and characterization of nanocrystalline polyhedral oligo silsesquioxanes (POSS) with cross-linkable functionalities. in Polyhedron. 2019;171:299-304.
doi:10.1016/j.poly.2019.06.059 .

Tomić, Nataša Z., Vuksanović, Marija M., Djokić, Veljko, Mitrić, Miodrag, Simić, Milena R., Pavlović, Vladimir, Jancić-Heinemann, Radmila, Marinković, Aleksandar D., "Synthesis and characterization of nanocrystalline polyhedral oligo silsesquioxanes (POSS) with cross-linkable functionalities" in Polyhedron, 171 (2019):299-304,
https://doi.org/10.1016/j.poly.2019.06.059 . .