TY  - JOUR
AU  - Nikolić, M.V.
AU  - Vasiljević, Zorka
AU  - Luković, M.D.
AU  - Pavlović, Vera P.
AU  - Krstić, J.B.
AU  - Vujancević, J.
AU  - Tadić, N.
AU  - Vlahović, Branislav
AU  - Pavlović, Vladimir
PY  - 2019
UR  - http://aspace.agrif.bg.ac.rs/handle/123456789/5136
AB  - Zinc ferrite nanocrystalline powder was obtained by solid state synthesis of starting zinc oxide and hematite nanopowders. Field emission scanning electron microscopy and transmission electron microscopy, X-ray diffraction, X-ray photoelectron spectroscopy and Raman spectroscopy confirmed the formation of nanocrystalline zinc-ferrite powder with a mixed spinel structure with small amounts of remaining zinc oxide and hematite as impurities. Thick film paste was formed and screen printed on test interdigitated PdAg electrodes on alumina substrate. Formation of a porous nanocrystalline structure was confirmed by scanning electron microscopy and Hg porosimetry. Humidity sensing properties of zinc ferrite thick films were investigated by monitoring the change in impedance in the relative humidity interval 30%-90% in the frequency range 42 Hz-1 MHz at room temperature (25°C) and 50°C. At 42 Hz at both analyzed temperatures the impedance reduced ~46 times in the humidity range 30%-90%. The dominant influence of grain boundaries was confirmed by analysis of complex impedance with an equivalent circuit.
PB  - Blackwell Publishing Ltd
T2  - International Journal of Applied Ceramic Technology
T1  - Investigation of ZnFe 2 O 4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing
EP  - 993
IS  - 3
SP  - 981
VL  - 16
DO  - 10.1111/ijac.13190
ER  - 

@article{
author = "Nikolić, M.V. and Vasiljević, Zorka and Luković, M.D. and Pavlović, Vera P. and Krstić, J.B. and Vujancević, J. and Tadić, N. and Vlahović, Branislav and Pavlović, Vladimir",
year = "2019",
abstract = "Zinc ferrite nanocrystalline powder was obtained by solid state synthesis of starting zinc oxide and hematite nanopowders. Field emission scanning electron microscopy and transmission electron microscopy, X-ray diffraction, X-ray photoelectron spectroscopy and Raman spectroscopy confirmed the formation of nanocrystalline zinc-ferrite powder with a mixed spinel structure with small amounts of remaining zinc oxide and hematite as impurities. Thick film paste was formed and screen printed on test interdigitated PdAg electrodes on alumina substrate. Formation of a porous nanocrystalline structure was confirmed by scanning electron microscopy and Hg porosimetry. Humidity sensing properties of zinc ferrite thick films were investigated by monitoring the change in impedance in the relative humidity interval 30%-90% in the frequency range 42 Hz-1 MHz at room temperature (25°C) and 50°C. At 42 Hz at both analyzed temperatures the impedance reduced ~46 times in the humidity range 30%-90%. The dominant influence of grain boundaries was confirmed by analysis of complex impedance with an equivalent circuit.",
publisher = "Blackwell Publishing Ltd",
journal = "International Journal of Applied Ceramic Technology",
title = "Investigation of ZnFe 2 O 4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing",
pages = "993-981",
number = "3",
volume = "16",
doi = "10.1111/ijac.13190"
}

Nikolić, M.V., Vasiljević, Z., Luković, M.D., Pavlović, V. P., Krstić, J.B., Vujancević, J., Tadić, N., Vlahović, B.,& Pavlović, V.. (2019). Investigation of ZnFe 2 O 4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing. in International Journal of Applied Ceramic Technology
Blackwell Publishing Ltd., 16(3), 981-993.
https://doi.org/10.1111/ijac.13190

Nikolić M, Vasiljević Z, Luković M, Pavlović VP, Krstić J, Vujancević J, Tadić N, Vlahović B, Pavlović V. Investigation of ZnFe 2 O 4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing. in International Journal of Applied Ceramic Technology. 2019;16(3):981-993.
doi:10.1111/ijac.13190 .

Nikolić, M.V., Vasiljević, Zorka, Luković, M.D., Pavlović, Vera P., Krstić, J.B., Vujancević, J., Tadić, N., Vlahović, Branislav, Pavlović, Vladimir, "Investigation of ZnFe 2 O 4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing" in International Journal of Applied Ceramic Technology, 16, no. 3 (2019):981-993,
https://doi.org/10.1111/ijac.13190 . .

TY  - JOUR
AU  - Nikolić, M.V.
AU  - Sekulić, D.L.
AU  - Nikolić, N.
AU  - Slankamenac, M.P.
AU  - Aleksić, O.S.
AU  - Danninger, H.
AU  - Halwax, E.
AU  - Pavlović, Vladimir
AU  - Nikolić, P.M.
PY  - 2013
UR  - http://aspace.agrif.bg.ac.rs/handle/123456789/3106
AB  - In this work we have analyzed the effects of Ti doping on structural and electrical properties of alpha-Fe2O3. When the amount of added Ti (5 wt.% TiO2) was within the solubility degree and XRD, SEM and EDS analysis revealed a homogenous hematite structure, with lattice parameters a= 5.03719(3), c= 13.7484(1) slightly increased due to incorporation of Ti into the rhombohedral hematite lattice. Higher amounts of Ti (10 wt.% TiO2) resulted in the formation of pseudobrookite, besides hematite, confirmed by SEM and EDS analysis. Studies of electric properties in the temperature range 25-225oC at different frequencies (100-1Mz) showed that Ti doping improved electrical conductivity. Impedance analysis was performed using an equivalent circuit, showing one relaxation process and suggesting dominant grain boundary contribution.
PB  - Međunarodni Institut za nauku o sinterovanju, Beograd
T2  - Science of Sintering
T1  - Structural and Electrical Properties of Ti Doped alpha-Fe2O3
EP  - 292
IS  - 3
SP  - 281
VL  - 45
DO  - 10.2298/SOS1303281N
ER  - 

@article{
author = "Nikolić, M.V. and Sekulić, D.L. and Nikolić, N. and Slankamenac, M.P. and Aleksić, O.S. and Danninger, H. and Halwax, E. and Pavlović, Vladimir and Nikolić, P.M.",
year = "2013",
abstract = "In this work we have analyzed the effects of Ti doping on structural and electrical properties of alpha-Fe2O3. When the amount of added Ti (5 wt.% TiO2) was within the solubility degree and XRD, SEM and EDS analysis revealed a homogenous hematite structure, with lattice parameters a= 5.03719(3), c= 13.7484(1) slightly increased due to incorporation of Ti into the rhombohedral hematite lattice. Higher amounts of Ti (10 wt.% TiO2) resulted in the formation of pseudobrookite, besides hematite, confirmed by SEM and EDS analysis. Studies of electric properties in the temperature range 25-225oC at different frequencies (100-1Mz) showed that Ti doping improved electrical conductivity. Impedance analysis was performed using an equivalent circuit, showing one relaxation process and suggesting dominant grain boundary contribution.",
publisher = "Međunarodni Institut za nauku o sinterovanju, Beograd",
journal = "Science of Sintering",
title = "Structural and Electrical Properties of Ti Doped alpha-Fe2O3",
pages = "292-281",
number = "3",
volume = "45",
doi = "10.2298/SOS1303281N"
}

Nikolić, M.V., Sekulić, D.L., Nikolić, N., Slankamenac, M.P., Aleksić, O.S., Danninger, H., Halwax, E., Pavlović, V.,& Nikolić, P.M.. (2013). Structural and Electrical Properties of Ti Doped alpha-Fe2O3. in Science of Sintering
Međunarodni Institut za nauku o sinterovanju, Beograd., 45(3), 281-292.
https://doi.org/10.2298/SOS1303281N

Nikolić M, Sekulić D, Nikolić N, Slankamenac M, Aleksić O, Danninger H, Halwax E, Pavlović V, Nikolić P. Structural and Electrical Properties of Ti Doped alpha-Fe2O3. in Science of Sintering. 2013;45(3):281-292.
doi:10.2298/SOS1303281N .

Nikolić, M.V., Sekulić, D.L., Nikolić, N., Slankamenac, M.P., Aleksić, O.S., Danninger, H., Halwax, E., Pavlović, Vladimir, Nikolić, P.M., "Structural and Electrical Properties of Ti Doped alpha-Fe2O3" in Science of Sintering, 45, no. 3 (2013):281-292,
https://doi.org/10.2298/SOS1303281N . .

TY  - JOUR
AU  - Nikolić, M.V.
AU  - Slankamenac, M.P.
AU  - Nikolić, N.
AU  - Sekulić, D.L.
AU  - Aleksić, O.S.
AU  - Mitrić, M.
AU  - Ivetić, T.
AU  - Pavlović, Vladimir
AU  - Nikolić, P.M.
PY  - 2012
UR  - http://aspace.agrif.bg.ac.rs/handle/123456789/3049
AB  - The effects of Zn-doping on the dielectric behavior and electrical properties of bulk alpha-Fe2O3 have been studied. X-ray diffraction analysis revealed the presence of two phases in all samples: hematite and spinel ZnFe2O4, with the amount of spinel phase increasing with increasing Zn content. Scanning electron microscopy analysis combined with energy dispersive X-ray spectroscopy showed that the Zn-bearing phase occurred in the form of individual spinel ZnFe2O4 grains in a hematite matrix. DC conductivity was measured in the temperature range 25-225 degrees C (298-498 K). Impedance spectroscopy measurements in the same temperature range were carried out in the frequency range 100Hz to 10 MHz. Increase in the Zn content resulted in increased electrical conductivity and higher values of the dielectric constant. The resistance and capacitance of grains and grain boundaries were analyzed by modeling the experimental results using an equivalent circuit.
PB  - Međunarodni Institut za nauku o sinterovanju, Beograd
T2  - Science of Sintering
T1  - Study of Dielectric Behavior and Electrical Properties of Hematite alpha-Fe2O3 Doped with Zn
EP  - 321
IS  - 3
SP  - 307
VL  - 44
DO  - 10.2298/SOS1203307N
ER  - 

@article{
author = "Nikolić, M.V. and Slankamenac, M.P. and Nikolić, N. and Sekulić, D.L. and Aleksić, O.S. and Mitrić, M. and Ivetić, T. and Pavlović, Vladimir and Nikolić, P.M.",
year = "2012",
abstract = "The effects of Zn-doping on the dielectric behavior and electrical properties of bulk alpha-Fe2O3 have been studied. X-ray diffraction analysis revealed the presence of two phases in all samples: hematite and spinel ZnFe2O4, with the amount of spinel phase increasing with increasing Zn content. Scanning electron microscopy analysis combined with energy dispersive X-ray spectroscopy showed that the Zn-bearing phase occurred in the form of individual spinel ZnFe2O4 grains in a hematite matrix. DC conductivity was measured in the temperature range 25-225 degrees C (298-498 K). Impedance spectroscopy measurements in the same temperature range were carried out in the frequency range 100Hz to 10 MHz. Increase in the Zn content resulted in increased electrical conductivity and higher values of the dielectric constant. The resistance and capacitance of grains and grain boundaries were analyzed by modeling the experimental results using an equivalent circuit.",
publisher = "Međunarodni Institut za nauku o sinterovanju, Beograd",
journal = "Science of Sintering",
title = "Study of Dielectric Behavior and Electrical Properties of Hematite alpha-Fe2O3 Doped with Zn",
pages = "321-307",
number = "3",
volume = "44",
doi = "10.2298/SOS1203307N"
}

Nikolić, M.V., Slankamenac, M.P., Nikolić, N., Sekulić, D.L., Aleksić, O.S., Mitrić, M., Ivetić, T., Pavlović, V.,& Nikolić, P.M.. (2012). Study of Dielectric Behavior and Electrical Properties of Hematite alpha-Fe2O3 Doped with Zn. in Science of Sintering
Međunarodni Institut za nauku o sinterovanju, Beograd., 44(3), 307-321.
https://doi.org/10.2298/SOS1203307N

Nikolić M, Slankamenac M, Nikolić N, Sekulić D, Aleksić O, Mitrić M, Ivetić T, Pavlović V, Nikolić P. Study of Dielectric Behavior and Electrical Properties of Hematite alpha-Fe2O3 Doped with Zn. in Science of Sintering. 2012;44(3):307-321.
doi:10.2298/SOS1203307N .

Nikolić, M.V., Slankamenac, M.P., Nikolić, N., Sekulić, D.L., Aleksić, O.S., Mitrić, M., Ivetić, T., Pavlović, Vladimir, Nikolić, P.M., "Study of Dielectric Behavior and Electrical Properties of Hematite alpha-Fe2O3 Doped with Zn" in Science of Sintering, 44, no. 3 (2012):307-321,
https://doi.org/10.2298/SOS1203307N . .

TY  - JOUR
AU  - Obradović, N.
AU  - Nikolić, M.V.
AU  - Nikolić, N.
AU  - Filipović, Suzana
AU  - Mitrić, M.
AU  - Pavlović, Vladimir
AU  - Nikolić, P.M.
AU  - Djordjević, Antonije
AU  - Ristić, M.M.
PY  - 2012
UR  - http://aspace.agrif.bg.ac.rs/handle/123456789/3052
AB  - Mixtures of BaCO3, ZnO and TiO2 powders, with molar ratio of 1:2:4, were mechanically activated for 20, 40 and minutes in a planetary ball mill. The resulting powders were compacted into pellets and isothermally sintered at 1250 degrees C for 2h with a heating rate of 10 degrees C/min. X-ray diffraction analysis of obtained powders and sintered samples was performed in order to investigate changes of the phase composition. The microstructure of sintered samples was examined by scanning electron microscopy. The photoacoustic phase and amplitude spectra of sintered samples were measured as a function of the laser beam modulating frequency using a transmission detection configuration. Fitting of experimental data enabled determination of photoacoustic properties including thermal diffusivity. Based on the results obtained correlation between thermal diffusivity and experimental conditions, as well the samples microstructure characteristics, was discussed.
PB  - Međunarodni Institut za nauku o sinterovanju, Beograd
T2  - Science of Sintering
T1  - Synthesis of Barium-zinc-titanate Ceramics
EP  - 71
IS  - 1
SP  - 65
VL  - 44
DO  - 10.2298/SOS1201065O
ER  - 

@article{
author = "Obradović, N. and Nikolić, M.V. and Nikolić, N. and Filipović, Suzana and Mitrić, M. and Pavlović, Vladimir and Nikolić, P.M. and Djordjević, Antonije and Ristić, M.M.",
year = "2012",
abstract = "Mixtures of BaCO3, ZnO and TiO2 powders, with molar ratio of 1:2:4, were mechanically activated for 20, 40 and minutes in a planetary ball mill. The resulting powders were compacted into pellets and isothermally sintered at 1250 degrees C for 2h with a heating rate of 10 degrees C/min. X-ray diffraction analysis of obtained powders and sintered samples was performed in order to investigate changes of the phase composition. The microstructure of sintered samples was examined by scanning electron microscopy. The photoacoustic phase and amplitude spectra of sintered samples were measured as a function of the laser beam modulating frequency using a transmission detection configuration. Fitting of experimental data enabled determination of photoacoustic properties including thermal diffusivity. Based on the results obtained correlation between thermal diffusivity and experimental conditions, as well the samples microstructure characteristics, was discussed.",
publisher = "Međunarodni Institut za nauku o sinterovanju, Beograd",
journal = "Science of Sintering",
title = "Synthesis of Barium-zinc-titanate Ceramics",
pages = "71-65",
number = "1",
volume = "44",
doi = "10.2298/SOS1201065O"
}

Obradović, N., Nikolić, M.V., Nikolić, N., Filipović, S., Mitrić, M., Pavlović, V., Nikolić, P.M., Djordjević, A.,& Ristić, M.M.. (2012). Synthesis of Barium-zinc-titanate Ceramics. in Science of Sintering
Međunarodni Institut za nauku o sinterovanju, Beograd., 44(1), 65-71.
https://doi.org/10.2298/SOS1201065O

Obradović N, Nikolić M, Nikolić N, Filipović S, Mitrić M, Pavlović V, Nikolić P, Djordjević A, Ristić M. Synthesis of Barium-zinc-titanate Ceramics. in Science of Sintering. 2012;44(1):65-71.
doi:10.2298/SOS1201065O .

Obradović, N., Nikolić, M.V., Nikolić, N., Filipović, Suzana, Mitrić, M., Pavlović, Vladimir, Nikolić, P.M., Djordjević, Antonije, Ristić, M.M., "Synthesis of Barium-zinc-titanate Ceramics" in Science of Sintering, 44, no. 1 (2012):65-71,
https://doi.org/10.2298/SOS1201065O . .